FIVE
­
1
Revision
4
August
2002
CHAPTER
FIVE
MISCELLANEOUS
TEST
METHODS
Prior
to
employing
the
methods
in
this
chapter,
analysts
are
advised
to
consult
the
disclaimer
statement
at
the
front
of
this
manual
and
the
information
in
Chapter
Two
for
guidance
on
the
allowed
flexibility
in
the
choice
of
apparatus,
reagents,
and
supplies.
(
Note:
Procedures
for
required
method­
defined
parameters
are
not
subject
to
the
same
flexibility
afforded
in
other
SW­
846
methods.)
In
addition,
unless
specified
in
a
regulation,
the
use
of
SW­
846
methods
is
not
mandatory
in
response
to
Federal
testing
requirements.
The
information
contained
in
each
procedure
is
provided
by
EPA
as
guidance
to
be
used
by
the
analyst
and
the
regulated
community
in
making
judgements
necessary
to
meet
the
data
quality
objectives
or
needs
for
the
intended
use
of
the
data.

The
following
methods
are
found
in
Chapter
Five:

Method
5050:
Bomb
Preparation
Method
for
Solid
Waste
Method
9010C:
Total
and
Amenable
Cyanide:
Distillation
Method
9012B:
Total
and
Amenable
Cyanide
(
Automated
Colorimetric,
with
Off­
Line
Distillation)
Method
9013:
Cyanide
Extraction
Procedure
for
Solids
and
Oils
Method
9014:
Titrimetric
and
Manual
Spectrophotometric
Determinative
Methods
for
Cyanide
Method
9020B:
Total
Organic
Halides
(
TOX)
Method
9021:
Purgeable
Organic
Halides
(
POX)
Method
9022:
Total
Organic
Halides
(
TOX)
by
Neutron
Activation
Analysis
Method
9023:
Extractable
Organic
Halides
(
EOX)
in
Solids
Method
9030B:
Acid­
Soluble
and
Acid­
Insoluble
Sulfides:
Distillation
Method
9031:
Extractable
Sulfides
Method
9034:
Titrimetric
Procedure
for
Acid­
Soluble
and
Acid­
Insoluble
Sulfides
Method
9035:
Sulfate
(
Colorimetric,
Automated,
Chloranilate)
Method
9036:
Sulfate
(
Colorimetric,
Automated,
Methylthymol
Blue,
AA
II)
Method
9038:
Sulfate
(
Turbidimetric)
Method
9056:
Determination
of
Inorganic
Anions
by
Ion
Chromatography
Method
9057:
Determination
of
Chloride
from
HCl/
Cl
2
Emission
Sampling
Train
(
Methods
0050
and
0051)
by
Anion
Chromatography
Method
9060A:
Total
Organic
Carbon
Method
9065:
Phenolics
(
Spectrophotometric,
Manual
4­
AAP
with
Distillation)
Method
9066:
Phenolics
(
Colorimetric,
Automated
4­
AAP
with
Distillation)
Method
9067:
Phenolics
(
Spectrophotometric,
MBTH
with
Distillation)
Method
9070A:
n­
Hexane
Extractable
Material
(
HEM)
for
Aqueous
Samples
Method
9071B:
n­
Hexane
Extractable
Material
(
HEM)
for
Sludge,
Sediment,
and
Solid
Samples
Method
9075:
Test
Method
for
Total
Chlorine
in
New
and
Used
Petroleum
Products
by
X­
Ray
Fluorescence
Spectrometry
(
XRF)
FIVE
­
2
Revision
4
August
2002
Method
9076:
Test
Method
for
Total
Chlorine
in
New
and
Used
Petroleum
Products
by
Oxidative
Combustion
and
Microcoulometry
Method
9077:
Test
Methods
for
Total
Chlorine
in
New
and
Used
Petroleum
Products
(
Field
Test
Kit
Methods)
Method
A:
Fixed
End
Point
Test
Kit
Method
Method
B:
Reverse
Titration
Quantitative
End
Point
Test
Kit
Method
Method
C:
Direct
Titration
Quantitative
End
Point
Test
Kit
Method
Method
9131:
Total
Coliform:
Multiple
Tube
Fermentation
Technique
Method
9132:
Total
Coliform:
Membrane­
Filter
Technique
Method
9210:
Potentiometric
Determination
of
Nitrate
in
Aqueous
Samples
with
Ion­
Selective
Electrode
Method
9211:
Potentiometric
Determination
of
Bromide
in
Aqueous
Samples
with
Ion­
Selective
Electrode
Method
9212:
Potentiometric
Determination
of
Chloride
in
Aqueous
Samples
with
Ion­
Selective
Electrode
Method
9213:
Potentiometric
Determination
of
Cyanide
in
Aqueous
Samples
and
Distillates
with
Ion­
Selective
Electrode
Method
9214:
Potentiometric
Determination
of
Fluoride
in
Aqueous
Samples
with
Ion­
Selective
Electrode
Method
9215:
Potentiometric
Determination
of
Sulfide
in
Aqueous
Samples
and
Distillates
with
Ion­
Selective
Electrode
Method
9250:
Chloride
(
Colorimetric,
Automated
Ferricyanide
AAI)
Method
9251:
Chloride
(
Colorimetric,
Automated
Ferricyanide
AAII)
Method
9253:
Chloride
(
Titrimetric,
Silver
Nitrate)
Method
9320:
Radium­
228
