10
­
2
0
2
4Metals,
Method
1620Metals,
1620
CADMIUM,
UG/
LCADMIUM,
L
calibration:
1calibration:
1
Standardized
Residuals
vs
Spike
ConcentrationEpisode
6000
DataPage
1
of
3APPENDIX
B
­
6
­
3
Standardized
Residuals
Log­
10
of
Spike
Concentration
no
valid
MLE
estimate
Metals,
Method
1620Metals,
1620
CADMIUM,
UG/
LCADMIUM,
L
calibration:
3calibration:
3
10
­
4
­
2
0
2
4
Metals,
Method
1620Metals,
1620
CHROMIUM,
UG/
LCHROMIUM,
L
calibration:
1calibration:
1
0.1
­
2
0
2
4Metals,
Method
1620Metals,
1620
CHROMIUM,
UG/
LCHROMIUM,
L
calibration:
3calibration:
3
100
­
2
0
2
4Metals,
Method
1620Metals,
1620
LEAD,
UG/
LLEAD,
L
calibration:
1calibration:
1
1
­
2
­
1
0
1
2
3Metals,
Method
1620Metals,
1620
LEAD,
UG/
LLEAD,
L
calibration:
3calibration:
3
100
­
2
­
1
0
1
2
Metals,
Method
1620Metals,
1620
MOLYBDENUM,
UG/
LMOLYBDENUM,
L
calibration:
1calibration:
1
100
­
1
0
1
2Metals,
Method
1620Metals,
1620
TIN,
UG/
LTIN,
L
calibration:
1calibration:
1
1
­
2
­
1
0
1
2
Metals,
Method
1620Metals,
1620
TIN,
UG/
LTIN,
L
calibration:
3calibration:
3
1001000
­
2
­
1
0
1
2
Metals,
Method
200.8Metals,
200.8
ALUMINUM,
UG/
LALUMINUM,
L
calibration:
1calibration:
1
110
­
2
0
2
4Metals,
Method
200.8Metals,
200.8
ALUMINUM,
UG/
LALUMINUM,
L
calibration:
3calibration:
3
10
­
2
­
1
0
1
2
Metals,
Method
200.8Metals,
200.8
ANTIMONY,
UG/
LANTIMONY,
L
calibration:
1calibration:
1
1
10100
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
ARSENIC,
UG/
LARSENIC,
L
calibration:
1calibration:
1
Standardized
Residuals
vs
Spike
ConcentrationEpisode
6000
DataPage
2
of
3
Standardized
Residuals
Log­
10
of
Spike
Concentration
0.11
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
ARSENIC,
UG/
LARSENIC,
L
calibration:
2calibration:
2
10
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
BARIUM,
UG/
LBARIUM,
L
calibration:
1calibration:
1
0.1
­
3
­
2
­
1
0
1
2
3
Metals,
Method
200.8Metals,
200.8
BARIUM,
UG/
LBARIUM,
L
calibration:
2calibration:
2
0.11
­
3
­
2
­
1
0
1
2
3
Metals,
Method
200.8Metals,
200.8
BERYLLIUM,
UG/
LBERYLLIUM,
L
calibration:
1calibration:
1
0.01
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
BERYLLIUM,
UG/
LBERYLLIUM,
L
calibration:
2calibration:
2
10
­
6
­
4
­
2
0
2
4
6
Metals,
Method
200.8Metals,
200.8
CHROMIUM,
UG/
LCHROMIUM,
L
calibration:
1calibration:
1
0.1
­
4
­
2
0
2
4
Metals,
Method
200.8Metals,
200.8
CHROMIUM,
UG/
LCHROMIUM,
L
calibration:
2calibration:
2
0.11
­
2
0
2
4Metals,
Method
200.8Metals,
200.8
COBALT,
UG/
LCOBALT,
L
calibration:
1calibration:
1
10
­
3
­
2
­
1
0
1
2
3
Metals,
Method
200.8Metals,
200.8
COPPER,
UG/
LCOPPER,
L
calibration:
1calibration:
1
0.1
­
6
­
4
­
2
0
2
4
6
Metals,
Method
200.8Metals,
200.8COPPER,
UG/
LCOPPER,
L
calibration:
2calibration:
2
10
­
2
­
1
0
1
2
Metals,
Method
200.8Metals,
200.8
LEAD,
UG/
LLEAD,
L
calibration:
1calibration:
1
1
1
11
0.1
­
4
­
2
0
2
4
Metals,
Method
200.8Metals,
200.8
LEAD,
UG/
LLEAD,
L
calibration:
2calibration:
2
Standardized
Residuals
vs
Spike
ConcentrationEpisode
6000
DataPage
3
of
3
Standardized
Residuals
Log­
10
of
Spike
Concentration
110
­
0.5
0.0
0.5
1.0Metals,
Method
200.8Metals,
200.8
MERCURY,
UG/
LMERCURY,
L
calibration:
1calibration:
1
10
­
5
0
5
Metals,
Method
200.8Metals,
200.8NICKEL,
UG/
LNICKEL,
L
calibration:
1calibration:
1
0.010.1
­
6
­
4
­
2
0
2
4
6
Metals,
Method
200.8Metals,
200.8
NICKEL,
UG/
LNICKEL,
L
calibration:
2calibration:
2
10100
­
4
­
2
0
2
4
Metals,
Method
200.8Metals,
200.8
SELENIUM,
UG/
LSELENIUM,
L
calibration:
1calibration:
1
0.11
­
4
­
2
0
2
4
Metals,
Method
200.8Metals,
200.8
SELENIUM,
UG/
LSELENIUM,
L
calibration:
2calibration:
2
10100
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
VANADIUM,
UG/
LVANADIUM,
L
calibration:
1calibration:
1
1
­
2
­
1
0
1
2
3Metals,
Method
200.8Metals,
200.8
VANADIUM,
UG/
LVANADIUM,
L
calibration:
2calibration:
2
10100
­
3
­
2
­
1
0
1
2
3
Metals,
Method
200.8Metals,
200.8
ZINC,
UG/
LZINC,
L
calibration:
1calibration:
1
1
­
4
­
2
0
2
4
Metals,
Method
200.8Metals,
200.8ZINC,
UG/
LZINC,
L
calibration:
2calibration:
2
1
